produce ester: let's make ethyl butanoate
1) Add 30 ml Ethanol and 20 ml butanoic acid to a round bottomed flask. Excess of the ethanol is added coz it's cheaper #cheapos
2) Add 5ml of concentrated sulphuric acid (as a dehydrating agent to shift the equilibrium in the forward direction --> increas yield of ester AND it's a catalyst so it increases the rate of the reaction making it go faster) and add some ceramic boiling chips (anti bumping granules to allow the even heating of the liquid and to increase surface area for vaporisation to occur on)
3) Attach a condenser to the the round bottomed flask with the reactants and stuff in it (used because the system is in equilibrium and if the reactants evaporate then like the equilibrium will shift in the reverse direction and reduce yield of ester which is bad). The round bottomed flask is placed in a water bath to allow even heating of water BUT a better thing to use is the heat plate because the reactants are volatile. I think in hsc we should write that we used a heat plate lol. cheap schools.
4) Anyway next put the Bunsen Burner on top of a heat mat and put it under the reaction vessel. (or use the heat plate)
5) Pass the cooling water through the condenser so it condenses the reactants, preventing evaporation and preventing the equilibrium from shifting to the left. Turn on Bunsen burner and the reaction occurs for half an hour at 100 degrees Celsius.
6) then after 30 mins, turn off the Bunsen burner and let the cooling water pass through for a while. after it's cooled, take the round bottomed flask and pour the ester mixture into a separating funnel. 20 ml of NAHCO3 was added to the separaring funnel, this is because NaHCO3 is amphiprotic and it acts as a base :. neutralising the excess butanoic acid which may remain unused in the reaction. The mixture was shaken and left to stand. The lower aqueous layer was drained off.
7) then add 20ml of DISTILLED WATER to the separating funnel. Since water is a polar substance, it would dissolve the excess polar ethanol if there is any because likes dissolve likes. Again shake it and drain off the lower aqueous layer leaving only the ester and you've successfully purified the ester ethyl butanoate (I hope
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Pretend I drew the diagram and the equilibrium equation for refluxing
k done
now mark it